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Beilstein J. Org. Chem. 2018, 14, 182–186, doi:10.3762/bjoc.14.12
Graphical Abstract
Scheme 1: Phthalide and fluorinated phthalides (1).
Scheme 2: Plausible reaction mechanism for the formation of phthalide 1a.
Scheme 3: Synthesis of fluorinated phthalides 1.
Scheme 4: Asymmetric synthesis of 1a using a chiral auxiliary.
Scheme 5: Catalytic asymmetric synthesis of 1a.
Beilstein J. Org. Chem. 2013, 9, 1663–1667, doi:10.3762/bjoc.9.190
Figure 1: Action spectrum of bromination with CBr4, induced by LED irradiation (red line), and absorption spe...
Scheme 1: Plausible mechanism for bromination of cyclohexane with CBr4 induced by LED irradiation.
Figure 2: 13C NMR monitoring of reaction mixtures: (a) 0.50 mmol of CBr4, 0.10 mL of cyclohexane, and 0.40 mL...